![一种三氯氢硅还原生产多晶硅循环氢气提纯处理方法](/CN/2011/1/40/images/201110200460.jpg)
基本信息:
- 专利标题: 一种三氯氢硅还原生产多晶硅循环氢气提纯处理方法
- 专利标题(英):Recycling hydrogen purification processing method for producing polysilicon by reducing trichlorosilane
- 申请号:CN201110200460.5 申请日:2011-07-18
- 公开(公告)号:CN102328906A 公开(公告)日:2012-01-25
- 发明人: 徐恒泳 , 唐春华 , 孙剑 , 董恩宁 , 侯守福
- 申请人: 中国科学院大连化学物理研究所
- 申请人地址: 辽宁省大连市中山路457号
- 专利权人: 中国科学院大连化学物理研究所
- 当前专利权人: 中国科学院大连化学物理研究所
- 当前专利权人地址: 辽宁省大连市中山路457号
- 代理机构: 沈阳科苑专利商标代理有限公司
- 代理人: 马驰
- 主分类号: C01B3/56
- IPC分类号: C01B3/56
The invention discloses a recycling hydrogen purification processing method for producing polysilicon by reducing trichlorosilane. Two groups of metal palladium composite membrane hydrogen purifiers which are serially connected are adopted for carrying out purification processing on recycling hydrogen obtained by trichlorosilane reduction, wherein the first group of metal palladium composite membrane hydrogen purifiers are relatively larger, the ultra-pure hydrogen (H2 purity is more than 99.9999%) after purification processing is returned to a reducing furnace and used as a raw material gas for trichlorosilane reduction; and the second group of hydrogen purifiers are relatively smaller, and the high-pure hydrogen (H2 purity is 99.999%) after purification processing is transmitted to a hydrogen cooling chemical section and used as a raw material gas. The recovery ratio of the recycling hydrogen after the purification processing by adopting the method disclosed by the invention can reach 99%. When hydrogen chloride content is higher in the recycling hydrogen, a necessary dechlorination measure is adopted for lowering HCl content below 0.5 ppm. By adopting the hydrogen purified by the method disclosed by the invention to produce the polysilicon, purity and quality of the polysilicon products can be obviously improved, and an obvious energy-saving emission reduction effect is achieved.
公开/授权文献:
- CN102328906B 一种三氯氢硅还原生产多晶硅循环氢气提纯处理方法 公开/授权日:2014-02-12
IPC结构图谱:
C | 化学;冶金 |
--C01 | 无机化学 |
----C01B | 非金属元素;其化合物 |
------C01B3/00 | 氢;含氢混合气;从含氢混合气中分离氢(用物理方法分离气体入B01D);氢的净化 |
--------C01B3/02 | .氢或含氢混合气的生产 |
----------C01B3/56 | ..用固体接触法;所用固体的再生 |