基本信息:
- 专利标题： 一种用微波-超声波协同催化制备烷基糖苷的方法
- 专利标题（英）：Method for preparing alkyl polyglucoside (APG) through microwave-ultrasonic wave concerted catalysis
- 申请号：CN201110148105.8 申请日：2011-05-30
- 公开(公告)号：CN102250160A 公开(公告)日：2011-11-23
- 发明人： 周大鹏 , 方银军 , 黄亚茹 , 葛赞 , 吴红平
- 申请人： 浙江赞宇科技股份有限公司
- 申请人地址： 浙江省杭州市上城区城头巷128号
- 专利权人： 浙江赞宇科技股份有限公司
- 当前专利权人： 赞宇科技集团股份有限公司,杭州赞宇化工有限公司
- 当前专利权人地址： 310000 浙江省杭州市城头巷128号
- 代理机构： 杭州九洲专利事务所有限公司
- 代理人： 王洪新
- 主分类号： C07H15/02
- IPC分类号： C07H15/02 ; C07H1/00
The invention relates to a method for preparing alkyl polyglucoside (APG) through microwave-ultrasonic wave concerted catalysis, and aims to provide a method having the advantages of high reaction speed, high conversion rate, small environmental influence and the like. The technical scheme comprises the following steps: a, adding glucose and fatty alcohol into a container according to a mol ratio of 1:(2-10), stirring, carrying out microwave heating for 5 minutes under ultrasonic wave radiation conditions to 110-120 DEG C, and carrying out vacuum dewatering for 15 minutes at the absolute pressure of 1.5-6.5 KPa; b, adding an acidic catalyst, and reacting for 30-90 minutes at the absolute pressure of 1.5-6.5 KPa; c, when the temperature is cooled to 50-80 DEG C after the reaction, neutralizing the acidic catalyst with a neutralizer until the pH value is 8-11; and d, raising the temperature to 120-200 DEG C, and carrying out reduced pressure distillation for dealcoholization at the absolute pressure of 1.5-6.5 KPa, thus obtaining a crude APG product.
公开/授权文献:
- CN102250160B 一种用微波-超声波协同催化制备烷基糖苷的方法 公开/授权日：2013-12-18
IPC结构图谱:
| C | 化学；冶金 |
| --C07 | 有机化学 |
| ----C07H | 糖类；及其衍生物；核苷；核苷酸；核酸 |
| ------C07H15/00 | 含有直接连在糖化物基团的杂原子上的烃基或取代烃基的化合物 |
| --------C07H15/02 | .未被环状结构取代的无环基团 |