![用铬渣制备氢氧化铬、氯化铅及混合硝酸盐的方法](/CN/2010/1/119/images/201010598010.jpg)
基本信息:
- 专利标题: 用铬渣制备氢氧化铬、氯化铅及混合硝酸盐的方法
- 专利标题(英):Method for preparing chromium hydroxide, lead chloride and mixed nitrate from chromium slag
- 申请号:CN201010598010.1 申请日:2010-12-21
- 公开(公告)号:CN102249313A 公开(公告)日:2011-11-23
- 发明人: 王嘉兴
- 申请人: 王嘉兴
- 申请人地址: 广东省东莞市东城区主山乌石岗村小学路1巷6号
- 专利权人: 王嘉兴
- 当前专利权人: 王嘉兴
- 当前专利权人地址: 广东省东莞市东城区主山乌石岗村小学路1巷6号
- 代理机构: 广州三环专利代理有限公司
- 代理人: 张艳美; 郝传鑫
- 主分类号: C01G37/00
- IPC分类号: C01G37/00 ; C01G21/16 ; C01F11/36 ; C01F5/38 ; C01F7/66 ; B09B3/00
The invention provides a method for preparing chromium hydroxide, lead chloride and mixed nitrate from chromium slag. Chromium slag is reacted with hydrochloric acid to obtain a mixed chloride of chromium chloride, calcium chloride, magnesium chloride and aluminium chloride. The reactant is treated with extraction filtration to obtain mixed chloride and a filter cake containing silica. The mixed chloride is added with excess industrial water, so that chromium chloride is hydrolyzed to trivalent chromium hydroxide which is precipitated; and extraction filtration is carried out to obtain clear calcium, magnesium and aluminium mixed chloride and a chromium hydroxide filter cake. The chromium hydroxide filter cake is washed, dried and crushed to obtain a chromium hydroxide product. The calcium, magnesium and aluminium mixed chloride is reacted with a lead nitrate solution to generate lead chloride and calcium, magnesium and aluminium mixed nitrate. A calcium, magnesium and aluminium mixed nitrate solution is treated with reduced pressure distillation, cooled and crystallized to obtain a calcium, magnesium and aluminium mixed nitrate product. Lead chloride is washed, dried and crushed to obtain a lead product.