![1-氯-2-甲基-2-丙醇的制备方法](/CN/2011/1/23/images/201110115006.jpg)
基本信息:
- 专利标题: 1-氯-2-甲基-2-丙醇的制备方法
- 专利标题(英):Method for preparing 1-chloro-2-methyl-2-propanol
- 申请号:CN201110115006.X 申请日:2011-04-28
- 公开(公告)号:CN102229522A 公开(公告)日:2011-11-02
- 发明人: 杨建军 , 余魏峰
- 申请人: 宁波尖锋紫星生物科技有限公司
- 申请人地址: 浙江省宁波市鄞州区南部商务区利时大厦6-1室
- 专利权人: 宁波尖锋紫星生物科技有限公司
- 当前专利权人: 宁波尖锋紫星生物科技有限公司
- 当前专利权人地址: 浙江省宁波市鄞州区南部商务区利时大厦6-1室
- 代理机构: 宁波市鄞州甬致专利代理事务所
- 代理人: 代忠炯
- 主分类号: C07C31/36
- IPC分类号: C07C31/36 ; C07C29/04 ; B01J31/08
The invention discloses a method for preparing 1-chloro-2-methyl-2-propanol. The method disclosed by the invention is characterized by comprising the following preparation steps: filling cation exchange resins into a filling pipe, wherein the length of the filling pipe filled with the cation exchange resins is 0.1-100 meters and the diameter of the filling pipe is 0.1-0.5 meter; respectively adding a reaction raw material, namely 2-methyl-3-chloropropene and water to the filling pipe from two feed ports of the filling pipe; cooling the exterior of the filling pipe to 0-45 DEG C, wherein the flow rate of the 2-methyl-3-chloropropene is 0.5-20kg/h and the flow rate of the water is 1-100L/h; and receiving a reaction liquid which flows out of the pipe. The preparation method disclosed by the invention has the advantages that a reaction is completed in one step; the production cost is low; a large quantity of acid waste water is not generated; and the pollution and damage to an environment are reduced.
公开/授权文献:
- CN102229522B 1-氯-2-甲基-2-丙醇的制备方法 公开/授权日:2013-12-04