
基本信息:
- 专利标题: 无溶剂制备热塑性分散体的方法
- 专利标题(英):Method for the solvent-free production of thermoplastic dispersions
- 申请号:CN200980127655.2 申请日:2009-07-06
- 公开(公告)号:CN102099106A 公开(公告)日:2011-06-15
- 发明人: 彼得·特吕伯 , 多米尼克·Ph·特吕伯
- 申请人: 图柏乳剂化学公司
- 申请人地址: 瑞士拉姆森
- 专利权人: 图柏乳剂化学公司
- 当前专利权人: 图柏乳剂化学公司
- 当前专利权人地址: 瑞士拉姆森
- 代理机构: 北京集佳知识产权代理有限公司
- 代理人: 蔡胜有; 吴鹏章
- 优先权: 08160557.8 2008.07.16 EP
- 国际申请: PCT/EP2009/058471 2009.07.06
- 国际公布: WO2010/006941 EN 2010.01.21
- 进入国家日期: 2011-01-14
- 主分类号: B01J19/18
- IPC分类号: B01J19/18 ; C08J3/05
Disclosed is a method for the production of thermoplastic polymer dispersions, using a reaction vessel with a first volume and a secondary volume, wherein a first stirrer is located and operative in said first volume and a secondary stirrer is located and operative in said secondary volume, wherein the first volume is at least 20 times larger than the secondary volume, wherein the stirrers in both volumes are able to handle viscosities above of or equal to 1000 mpas. The method comprises the steps of a.) loading the first volume of the vessel with an initial amount of polymer, optionally water and optionally alkaline; b.) heating the vessel externally to a target process temperature in the range of 80-300 DEG C; c.) operating the first stirrer in the first volume for at least half an hour at a speed of in the range of 10-100 rpm; d.) adding water and optional alkaline to the first volume; e.) connecting the secondary volume to the first volume and operating the secondary stirrer in the secondary volume at a speed of above 1000 rpm and recycling the reaction product through said secondary stirrer while keeping the operating temperature essentially constant during a timespan in excess of the recycle ratio 3 of the primary and the secondary mixer to form the dispersion. Furthermore disclosed is a dispersion as obtainable using such a method and a reaction vessel for carrying out such a method.
公开/授权文献:
- CN102099106B 无溶剂制备热塑性分散体的方法 公开/授权日:2014-07-09