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基本信息:
- 专利标题: 搅拌釜间歇氢化制备间苯二甲胺的方法
- 专利标题(英):Method for preparing m-xylylenediamine by intermittent hydrogenation in stirred tank
- 申请号:CN201010150725.0 申请日:2010-04-20
- 公开(公告)号:CN101955432A 公开(公告)日:2011-01-26
- 发明人: 黄志文 , 李海娟 , 汪幼强 , 田晓宏
- 申请人: 南通泰禾化工有限公司
- 申请人地址: 江苏省南通市如东县洋口化学工业园区
- 专利权人: 南通泰禾化工有限公司
- 当前专利权人: 南通泰禾化工股份有限公司
- 当前专利权人地址: 江苏省南通市如东县洋口化学工业园区
- 代理机构: 南通市永通专利事务所
- 代理人: 葛雷
- 主分类号: C07C211/27
- IPC分类号: C07C211/27 ; C07C209/48
The invention discloses a method for preparing m-xylylenediamine by intermittent hydrogenation in stirred tank. The method comprises the following steps of: pre-adding a modified granular solid catalyst to a stirred reaction kettle, and pumping a mixture of meta- dicyanobenzene, a ternary mixed solvent and a secondary amine inhibitor at high pressure for intermittent hydrogenation reaction; pressing reaction liquid and carrying out solid-liquid filter separation by directly utilizing self pressure of the reaction kettle after the reaction is ended, and rectifying the separated reaction liquidto obtain a target product; and returning the catalyst and an additional new catalyst to a hydrogenation kettle with pressure for recycling. The invention can realize automation control of the m-xylylenediamine stirred kettle batch hydrogenation production process, and has the advantages of no regeneration of the catalyst, simple and convenient operation, high utilization of device, stable reaction, low temperature, short time, high reaction yield, and the like.
公开/授权文献:
- CN101955432B 搅拌釜间歇氢化制备间苯二甲胺的方法 公开/授权日:2013-02-13
IPC结构图谱:
C | 化学;冶金 |
--C07 | 有机化学 |
----C07C | 无环或碳环化合物 |
------C07C211/00 | 含有与碳架连接的氨基的化合物 |
--------C07C211/01 | .与非环碳原子连接的氨基 |
----------C07C211/26 | ..含至少1个六元芳环的不饱和碳架的 |
------------C07C211/27 | ...用饱和碳链与六元芳环连接的氨基 |