
基本信息:
- 专利标题: 一种测定无烟气烟草制品中非极性或弱极性香味成分释放率的方法
- 专利标题(英):Method for measuring release rate of non-polar or low-polar flavor component in smoke-free tobacco product
- 申请号:CN200910227274.3 申请日:2009-12-04
- 公开(公告)号:CN101718757B 公开(公告)日:2012-04-25
- 发明人: 宋瑜冰 , 宗永立 , 马骥 , 李鹏 , 张杰 , 彭书海
- 申请人: 中国烟草总公司郑州烟草研究院
- 申请人地址: 河南省郑州市高新区枫杨街2号
- 专利权人: 中国烟草总公司郑州烟草研究院
- 当前专利权人: 中国烟草总公司郑州烟草研究院
- 当前专利权人地址: 河南省郑州市高新区枫杨街2号
- 代理机构: 郑州中民专利代理有限公司
- 代理人: 姜振东
- 主分类号: G01N30/02
- IPC分类号: G01N30/02 ; G01N1/28
The invention discloses a method for measuring the release rate of a non-polar or low-polar flavor component in a smoke-free tobacco product, which is mainly used for determining the release rate of the non-polar or low-polar flavor component in the smoke-free tobacco product by performing preliminary treatment and apparatus analysis on the smoke-free tobacco product. The method specifically comprises the following steps: weighing two parts of equivalent smoke-free tobacco products, adding artificial saliva and a methylene dichloride standard substance solution respectively, sealing and oscillating the mixture, extracting saliva extract twice with the equivalent methylene dichloride standard substance solution, combining the extract liquors, drying the combined extract liquor for cold storage and then feeding a sample in a concentration way; performing separation and detection on an extracted component with GC and GC-MS, retrieving and determining the content of the non-polar or low-polar flavor component according to a retaining time and a mass spectrum database, and comparing the content of the extracted component in the saliva with the content of the directly extracted component of the methylene dichloride solution so as to obtain the release rate of the flavor extracted component of the smoke-free tobacco product. The method has the advantages of simple process, high analysis speed, good accuracy, unlimited sample physical state and the like.
公开/授权文献:
- CN101718757A 一种测定无烟气烟草制品中非极性或弱极性香味成分释放率的方法 公开/授权日:2010-06-02
IPC结构图谱:
G | 物理 |
--G01 | 测量;测试 |
----G01N | 借助于测定材料的化学或物理性质来测试或分析材料 |
------G01N30/00 | 利用吸附作用、吸收作用或类似现象,或者利用离子交换,例如色谱法将材料分离成各个组分,来测试或分析材料 |
--------G01N30/02 | .柱色谱法 |