![聚碳酸酯树脂的制造方法](/CN/2007/8/8/images/200780043073.jpg)
基本信息:
- 专利标题: 聚碳酸酯树脂的制造方法
- 专利标题(英):Process for production of polycarbonate resin
- 申请号:CN200780043073.7 申请日:2007-09-25
- 公开(公告)号:CN101541855A 公开(公告)日:2009-09-23
- 发明人: 高桥和幸 , 岩木光地 , 内村竜次
- 申请人: 三菱化学株式会社
- 申请人地址: 日本东京
- 专利权人: 三菱化学株式会社
- 当前专利权人: 三菱化学株式会社
- 当前专利权人地址: 日本东京
- 代理机构: 北京三友知识产权代理有限公司
- 代理人: 丁香兰
- 优先权: 340464/2006 2006.12.18 JP
- 国际申请: PCT/JP2007/068571 2007.09.25
- 国际公布: WO2008/075490 JA 2008.06.26
- 进入国家日期: 2009-05-20
- 主分类号: C08G64/30
- IPC分类号: C08G64/30
The invention aims at providing a process for the production of polycarbonate resin which is suppressed in discoloration and reduced in the content of crystalline foreign substance, gel, and so on. The invention relates to a process for the production of polycarbonate resin from raw materials, namely, an aromatic dihydroxyl compound and a carbonic diester through continuous transesterification by the use of a production unit provided with plural reactors, which comprises producing continuously an aromatic polycarbonate resin having a viscosity-average molecular weight of 10,000 to 20,000 for a prescribed time before the termination of the continuous transesterification, discharging the polymerization fluid, cleaning the insides of the reactors with a mixture of the raw materials and then with an aromatic dihydroxyl compound, feeding the raw materials and a catalyst to the reactors after the internal temperatures and degrees of vacuum of the reactors have reached respectively to levels falling within -5% to +5% of the levels preset for manufacturing operation, and then initiating manufacturing operation again.
IPC结构图谱:
C | 化学;冶金 |
--C08 | 有机高分子化合物;其制备或化学加工;以其为基料的组合物 |
----C08G | 用碳—碳不饱和键以外的反应得到的高分子化合物 |
------C08G64/00 | 由在高分子主链上形成碳酸酯键的反应制得的高分子化合物 |
--------C08G64/20 | .一般制备方法 |
----------C08G64/30 | ..使用碳酸酯类 |