![用酸化—萃取法从含硼氯化镁溶液中提取硼酸的方法](/CN/2009/1/27/images/200910138814.jpg)
基本信息:
- 专利标题: 用酸化—萃取法从含硼氯化镁溶液中提取硼酸的方法
- 专利标题(英):Method for extracting boric acid from boron-containing magnesium chloride solution by using an acidification-extraction method
- 申请号:CN200910138814.0 申请日:2009-04-29
- 公开(公告)号:CN101538048A 公开(公告)日:2009-09-23
- 发明人: 李宏灿 , 吴小王 , 魏新俊 , 谢云荣 , 赖学明 , 魏廷祥 , 刘必箐 , 朱海丽
- 申请人: 青海中信国安科技发展有限公司
- 申请人地址: 青海省格尔木市昆仑北路99号
- 专利权人: 青海中信国安科技发展有限公司
- 当前专利权人: 青海中信国安科技发展有限公司
- 当前专利权人地址: 青海省格尔木市昆仑北路99号
- 代理机构: 西宁正坤知识产权代理事务所
- 代理人: 姜艳华
- 主分类号: C01B35/10
- IPC分类号: C01B35/10
The invention belongs to the field of inorganic chemical technology, and particularly relates to a method for extracting boric acid from boron-containing magnesium chloride solution by using an acidification-extraction method. The method is characterized in that: (a) the process flows comprise acidification, filtering, and multiple extraction, and also have four processes, namely thermosol colorization, slag removal by filtration, cold crystallization filtration, and evaporation, and then a boric acid product is obtained after the crystallization filtration; and (b) the process conditions comprises that hydrochloric acid or sulfuric acid is added into boron-containing magnesium chloride brine in acidification, thereby leading the pH-value of brine to be 0-3; the acidification temperature is room temperature; the acidification time is 10-60 minutes; the mass percent of crude boric acid: industrial hydrogen peroxide: active carbon or fly ash in thermosol colorization is 100:0.01-5:0.5-5; and the heating temperature in thermosol colorization is 80-95 DEG C. The method is fully applicable to the industrial production need of the existing salt lake brine boron extract, greatly lowers the production cost and equipment investment, and lays down solid technology basis for the large-scale industrial salt lake brine extract.
IPC结构图谱:
C | 化学;冶金 |
--C01 | 无机化学 |
----C01B | 非金属元素;其化合物 |
------C01B35/00 | 硼;其化合物 |
--------C01B35/08 | .含硼和氮、磷、氧、硫、硒或碲的化合物 |
----------C01B35/10 | ..含硼和氧的化合物 |