
基本信息:
- 专利标题: 固态腰果酚及其制备方法
- 专利标题(英):Solid-state cardanol and preparation thereof
- 申请号:CN200810231235.6 申请日:2008-12-05
- 公开(公告)号:CN101412661B 公开(公告)日:2011-06-22
- 发明人: 刘国际 , 毛治博 , 张兴喜 , 雒廷亮
- 申请人: 郑州大学
- 申请人地址: 河南省郑州市高新技术开发区科学大道100号
- 专利权人: 郑州大学
- 当前专利权人: 郑州大学
- 当前专利权人地址: 河南省郑州市高新技术开发区科学大道100号
- 代理机构: 郑州联科专利事务所
- 代理人: 刘建芳
- 主分类号: C07C39/06
- IPC分类号: C07C39/06 ; C07C37/00
The invention provides solid cardanol. The component of the solid cardanol is cardanol of which the side chain is saturated. The preparation method for the solid cardanol comprises the following steps: putting the cardanol or cashew nut oil into an autoclave, adding catalyst into the autoclave, firstly introducing a protective gas to exhaust air in the autoclave, then introducing hydrogen, and stirring for reaction for 3 to 6 hours at a temperature of between 100 and 200 DEG C and atmospheric pressure of between 1 and 5 MPa; and after the reaction is finished, collecting the product, then decompressing and distilling the product, and cooling the distillate to obtain the solid cardanol. The solid cardanol has the following advantages that the side chain of the solid cardanol is saturated, so the side chain does not generate self-gathering during fine purification at high temperature or high temperature treatment process for synthesizing other products; the solid cardanol is not easily oxidized nor lost by self-gathering during storage and transportation; and the solid cardanol does not generate self-gathering during fine purification of decompression and distillation, so the yield of the solid cardanol is improved.
公开/授权文献:
- CN101412661A 固态腰果酚及其制备方法 公开/授权日:2009-04-22